1.02 g of salicylideneaniline 0.61 g total of NaBH4 0.59 g total end product Als
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1.02 g of salicylideneaniline 0.61 g total of NaBH4 0.59 g total end productAlso, what is the melting point of the product? And the source product) for he setuliu reaction scheme (starting material(s), reagents, expected step synthesi s. Solvents and catalysts should be included, though "work up" steps need not be shown. OH No BH ethanol 2-(Anilnomethyl) phenol Salicytidene anilin sIs Amounts of Starting Materials and Reagents Used List all starting materials and reagents used in the second step of your multi-step synthesis (solvents and catalysts need not be indicated). For starting materials and pure reagents, give the measured wei moles. For reagents used as solutions, give the measured volume used, the concentration of the solution, ght actually used as well as the number of of moles. urne | Goncentraten alicyI idenea1 02 9 NO BH4 0.0052 mo 0.21 0052 malmL ethanet glacial acencaud Melting Point Data H0 ieliuir naeting phtaforganic sarting maouce chemspidex 5 drop 20 mL 2 " Literature melting point of organic starting material: Suliclideneaniline Literature melting point of 2 starting material or reagent: (not all reactions will have a second solid starting material or reagent) Literature melting point of intended product: Source: 2-(Anilingmehpheno Experimental melting point of product obtained: Percent Yield Give both the weight and the percent yield of the product obtained and show your calculations. If no product was obained, check hereand show calculation of percent yield if 0.20 g of product had been obtaine (If no solid product obtained, check here Assessment Was the desired product obtained? Briefly explain why you believe the product was or was not obained. how you could determine by means of either IR or H NMR spectroscopy whether or not your reaction was a success Describe at least one specific peak (or set of peaks) that would be vice-versa. For example, if your reaction was the nitration of benzene to give nitrobenzene, you might say. "The p would have two large peaks at 1350 cm and 1550 cm in its IR spectrum that wouldn't be present in the starting material." (Use the back of this page for your answers to these questions) Also, expl uct but not the starting material
Explanation / Answer
Well here NaBH4 acts as a reducing agent and in this type of reaction these type of reagents should be present in abundance.
In your case you have
No. of moles of Salicylideneaniline = 1.02 / 197.23 = 5.17 m moles
No. of moles of NaBH4 = 0.61 / 37.83 = 16.1 m moles
In these reactions, all of the Salicylideneaniline will not be converted to 2-(Anilinomethyl) phenol.
So there is no limiting reagent.
Its melting point is not availble online although I guess you can find it in some research papers.
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