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Ligand X forms a complex with both cobalt and copper, each of which has a maximu

ID: 589721 • Letter: L

Question

Ligand X forms a complex with both cobalt and copper, each of which has a maximum absorbance at 510 nm and 645 nm, respectively. A 0.280-g sample containing volume of 100.0 mL: A solution containing ligand X was added to a 50.0 mL aliquot of the sample solution and diluted to a final volume of 100.0 mL. The measured absorbance of the unknown solution waS 0.416 at 510 nm and 0.304 at 645 nm, when measured with a 1.00-am cell. The molar absorptivities of the cobalt and copper complexes at each wavelength are shown in the table below cobalt and copper was dissolved and diluted to a wavelength A, nm 510 645 Molar Absorptivity (e, M-1cm-1) Co 3.7040 x101 1262 Cu 5617 17810 What is the concentration of cobalt and copper in the final diluted solution? Number Number What is the weight percent of cobalt (FM -58.933 gímol) and copper (FM -63.546 g/mol) in the 0.280-g Number Number I wt % Co2+-- % wt% Cu"-

Explanation / Answer

Absorbance of solution = absorbances of all components in solution

Absorbance = molar absorptivity x path length x concentration

with path length = 1 cm

we have,

at 510 nm,

0.416 = 3.704 x 10^4[Co] + 5617[Cu]

at 645 nm,

0.304 = 1262[Co] + 17810[Cu]

Solving,

Concentration of cobalt and cupper in final diluted solution,

[Co2+] = 8.74 x 10^-6 M

[Cu2+] = 1.64 x 10^-5 M

moles of Co2+ in original solution = 8.74 x 10^-6 M x 100 ml/50 ml = 1.75 x 10^-5 M x 0.1 L = 1.75 x 10^-6 mol

mass of Co2+ in original solution = 1.75 x 10^-6 mol x 58.933 g/mol = 0.000103 g

wt% Co2+ = 0.000103 g x 100/0.280 g = 0.037%

moles of Cu2+ in original solution = 1.64 x 10^-5 M x 100 ml/50 ml = 3.28 x 10^-5 M x 0.1 L = 3.28 x 10^-6 mol

mass of Cu2+ in original solution = 3.28 x 10^-6 mol x 63.546 g/mol = 0.00021 g

wt% Cu2+ = 0.00021 g x 100/0.280 g = 0.074%

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