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can someone help me make sense of these NMR? I have attached my 2 samples that w

ID: 988422 • Letter: C

Question

can someone help me make sense of these NMR? I have attached my 2 samples that were analyzed by NMR spectroscopy. Can someone help me make sense of it?

THIS IS THE PRODUCT

254 r 7.467 5.542 0.0 2.5 3.8 5.0 6.3 7.5 8.8 10.0 No. Ret. Time Peak Name Height Area Rel Area Amount Type U"mi 1.87 n.a 2.15 n.a. 14.414 6.546 15.69 21.571 1461 .38 3.41 0.276 0.898 0.85 16.231 .880 16.95 6.872 0.662 0.63 n.a. BMB n.a. BMB 2.41 a. 17.050 3.601 n.a.BM n.a 42.73 na. n.aMb n.a. bMB n.a. bMB MB n.a 2.88 a. n.a 5.54 n.a Total 869.387 105.471 100.00 0.000

Explanation / Answer

If you could provide NMR of both staring as well as product, it would be easy for me to compare.

Mass spectrum of both compound are attached so we can compare this.

Only one thing that we can point out is that retention time of both.

For starting material its 7.4 min

For product its = 6.8 min.

So we can conclude from this data, staring material is not present.

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