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1a. In mass spectrometry, the molecular ion peak is the ___ and tells you the __

ID: 938093 • Letter: 1

Question

1a. In mass spectrometry, the molecular ion peak is the ___ and tells you the ____.

tallest peak/bond types

(M)+• peak/molecular weight

(M+1)+• peak/base peak

1b. The HDI of C3H5ClO is:

0

1

2

3

1c. In H NMR, propane has ____ kind(s) of chemically equivalent proton(s) in a ratio of ____ to ___.

1/8/0

2/6/2

3/3/5

1d. In H NMR, which proton is the most deshielded?

C-H

H-C-Cl

O-H

1e. A two step synthesis of Naproxen is shown below. In the second step, a Grignard reagent reacts at

C-1 (carbonyl carbon)

C-2 (carbon bonded to Br)

C-3

1f. Note Reagent 2 has a –COOMgCl group instead of –COOH. The –COOMgCl is used because this reagent will not react with ___ whereas –COOH will.

Explanation / Answer

1a. In mass spectrometry, the molecular ion peak is the _(M)+• peak __ and tells you the molecular weight ____.

tallest peak/bond types

1b. The HDI of C3H5ClO is: what is HDI ? Is it IHD, ok I assume it as IHD-

IHD is 1

1c. In H NMR, propane has _2___ kind(s) of chemically equivalent proton(s) in a ratio of _6___ to 2___.

1d. In H NMR, which proton is the most deshielded?

O-H

1e. A two step synthesis of Naproxen is shown below. In the second step, a Grignard reagent reacts at

C-2 (carbon bonded to Br)

1f. Note Reagent 2 has a –COOMgCl group instead of –COOH. The –COOMgCl is used because this reagent will not react with Grignard reagent ___ whereas –COOH will.

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