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2. There has been done a study on the addition of ascorbic acid in the manufactu

ID: 3318391 • Letter: 2

Question

2. There has been done a study on the addition of ascorbic acid in the manufacture of dangke to identify the effect on the storage capacity based on the value of TBA. The research was conducted by using Completely Randomized Design (RAL) Factorial pattern: Factor A is level of addition of ascorbic acid (1%, 1.5%, and 296); and Factor B is the length of storage time (4 days, 5 days and 6 days). The result (TBA value) research obtained is presented in the following table. Faktor B 5hr 6.30 6.10 6.80 5.30 6.30 30.80 5.20 6.20 5.60 6.50 5.30 28.80 5.10 4.80 4.87 5.16 5.00 24.93 84.53 Faktor A TOTAL 4hr 5.20 5.10 5.30 5.00 5.20 25.80 5.00 5.10 4.90 6hr 6.68 6.71 6.73 6.76 6.78 33.66 5.90 6.00 6.30 5.77 5.52 29.48 5.10 18.18 17.91 18.83 17.06 18.28 90.26 16.10 17.30 16.80 17.13 15.92 S3.25 14.92 14.68 14.84 15.03 14.50 73.97 247.47 1% Sub Total 1.5% 5.10 24.96 4.72 4.78 4.77 4.67 4.70 23.64 74.40 Sub Total 5.20 5.20 4.80 25.40 88.54 2% Sub Total Use Minitab software to answer the questions below. a. Does the ascorbic acid addition rate affect the value of TBA? b. Does storage time affect the value of TBA? c. Is there an interaction between ascorbic acid level (Factor A) and storage time (Factor B) to the value of TBA obtained?

Explanation / Answer

Result:

General Linear Model: TBA versus A, B

Method

Factor coding

(-1, 0, +1)

Factor Information

Factor

Type

Levels

Values

A

Fixed

3

1.00%, 1.50%, 2.00%

B

Fixed

3

4hr, 5hr, 6hr

Analysis of Variance

Source

DF

Adj SS

Adj MS

F-Value

P-Value

A

2

8.903

4.45136

51.18

0.000

B

2

7.089

3.54444

40.75

0.000

A*B

4

1.957

0.48919

5.62

0.001

Error

36

3.131

0.08697

Total

44

21.079

To test effect of ascorbic acid, calculated F=51.18, P=0.000 which is significant at 5% level.

To test effect of storage time, calculated F=40.75, P=0.000 which is significant at 5% level.

To test effect of interaction, calculated F=5.62, P=0.001 which is significant at 5% level.

Model Summary

S

R-sq

R-sq(adj)

R-sq(pred)

0.294912

85.15%

81.85%

76.79%

Coefficients

Term

Coef

SE Coef

T-Value

P-Value

VIF

Constant

5.4996

0.0440

125.10

0.000

A

1.00%

0.5178

0.0622

8.33

0.000

1.33

1.50%

0.0504

0.0622

0.81

0.422

1.33

B

4hr

-0.5396

0.0622

-8.68

0.000

1.33

5hr

0.1358

0.0622

2.18

0.036

1.33

A*B

1.00% 4hr

-0.3178

0.0879

-3.61

0.001

1.78

1.00% 5hr

0.0069

0.0879

0.08

0.938

1.78

1.50% 4hr

-0.0184

0.0879

-0.21

0.835

1.78

1.50% 5hr

0.0742

0.0879

0.84

0.404

1.78

Regression Equation

TBA

=

5.4996 + 0.5178 A_1.00% + 0.0504 A_1.50% - 0.5682 A_2.00% - 0.5396 B_4hr + 0.1358 B_5hr
+ 0.4038 B_6hr - 0.3178 A*B_1.00% 4hr + 0.0069 A*B_1.00% 5hr + 0.3109 A*B_1.00% 6hr
- 0.0184 A*B_1.50% 4hr + 0.0742 A*B_1.50% 5hr - 0.0558 A*B_1.50% 6hr + 0.3362 A*B_2.00%
4hr - 0.0811 A*B_2.00% 5hr - 0.2551 A*B_2.00% 6hr

Fits and Diagnostics for Unusual Observations

Obs

TBA

Fit

Resid

Std Resid

8

6.800

6.160

0.640

2.43

R

9

5.300

6.160

-0.860

-3.26

R

21

5.200

5.760

-0.560

-2.12

R

24

6.500

5.760

0.740

2.81

R

R Large residual

MINITAB data

A

B

TBA

1%

4hr

5.2

1%

4hr

5.1

1%

4hr

5.3

1%

4hr

5

1%

4hr

5.2

1%

5hr

6.3

1%

5hr

6.1

1%

5hr

6.8

1%

5hr

5.3

1%

5hr

6.3

1%

6hr

6.68

1%

6hr

6.71

1%

6hr

6.73

1%

6hr

6.76

1%

6hr

6.78

1.50%

4hr

5

1.50%

4hr

5.1

1.50%

4hr

4.9

1.50%

4hr

4.86

1.50%

4hr

5.1

1.50%

5hr

5.2

1.50%

5hr

6.2

1.50%

5hr

5.6

1.50%

5hr

6.5

1.50%

5hr

5.3

1.50%

6hr

5.9

1.50%

6hr

6

1.50%

6hr

6.3

1.50%

6hr

5.77

1.50%

6hr

5.52

2%

4hr

4.72

2%

4hr

4.78

2%

4hr

4.77

2%

4hr

4.67

2%

4hr

4.7

2%

5hr

5.1

2%

5hr

4.8

2%

5hr

4.87

2%

5hr

5.16

2%

5hr

5

2%

6hr

5.1

2%

6hr

5.1

2%

6hr

5.2

2%

6hr

5.2

2%

6hr

4.8

Factor coding

(-1, 0, +1)

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