Fill in the following Reaction Table Reaction Tables Group Member 1 (from partI

Question

Fill in the following Reaction Table

Reaction Tables Group Member 1 (from partI in lab text) All possible products Ph PrOH +NaBH4 +enantiomer + enantiomer 210 40 60 212 214 214 mmol0.35 15 mg 0.5 mL amt mp or bp density (if liquid) 134-138C 146-149 C 137-139 °C Limiting yes/no yes/no Group Member 2 (from part I in lab text) All possible product:s PrOH + NaBH, racemic mixture +enantiomer + enantiomer MW 21 40 60 212 214 214 mmol 0.35 -15 mg 0.5 mL amt mp or bp density 134-138C 146-149 C 137-139 °C (if liquid) Limiting yes/no yes/no

Explanation / Answer

Reagents table

Group 1

             PhCOCOPh         +             NaBH4        in      iPrOH

MW              210                                   40                        60

mmol            0.35                                 0.375                 

amt              73.5mg                            15 mg                 0.5 ml

bp/mp            95 oC                                                       82.6 oC

density                                                                           0.786 g/ml

limiting            No                                 yes

reagent

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Group II

             PhCOC(OH)Ph         +             NaBH4        in      iPrOH

MW              212                                   40                        60

mmol            0.35                                 0.375                 

amt              74.2mg                            15 mg                 0.5 ml

bp/mp            95 oC                                                       82.6 oC

density                                                                           0.786 g/ml

limiting            No                                 yes

reagent

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